5SZP
Protocadherin Gamma B7 extracellular cadherin domains 1-4 P21 crystal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-22 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97919 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 83.813, 45.549, 127.072 |
Unit cell angles | 90.00, 96.91, 90.00 |
Refinement procedure
Resolution | 19.977 - 3.100 |
R-factor | 0.2586 |
Rwork | 0.256 |
R-free | 0.30980 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5szo |
RMSD bond length | 0.002 |
RMSD bond angle | 0.585 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.950 | 3.310 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.180 | 1.512 |
Number of reflections | 17677 | |
<I/σ(I)> | 5.5 | 0.8 |
Completeness [%] | 99.5 | 99.2 |
Redundancy | 3.4 | 3.3 |
CC(1/2) | 0.982 | 0.585 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 8.5 | 295 | 0.1 M Tris-Cl pH 8.5, 0.2 trimethylamine N-oxide, 5% (v/v) Jeffamine M-600 pH 7.0, 17% (w/v) PEG2000MME |