5SZF
2A10 FAB fragment 2.54 Angstoms
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-04-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.00000 |
Spacegroup name | I 41 3 2 |
Unit cell lengths | 204.213, 204.213, 204.213 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.284 - 2.520 |
R-factor | 0.2263 |
Rwork | 0.225 |
R-free | 0.24830 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.568 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.200 | 2.520 |
High resolution limit [Å] | 2.520 | |
Rmerge | 0.025 | 0.366 |
Number of reflections | 24796 | |
<I/σ(I)> | 24.1 | |
Completeness [%] | 100.0 | |
Redundancy | 2 | 2.61 |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | 2M Ammonium sulfate 0.1 M trisodium citrate pH 5.5 |