5SWS
Crystal Structure of NP2-B17 TCR-H2Db-NP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-11-05 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95370 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 48.017, 126.942, 80.479 |
Unit cell angles | 90.00, 105.66, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.100 | 49.100 | 3.010 |
High resolution limit [Å] | 2.860 | 9.040 | 2.860 |
Rmerge | 0.124 | 0.029 | 0.579 |
Rmeas | 0.169 | 0.073 | 0.043 |
Rpim | 0.081 | 0.035 | 0.022 |
Total number of observations | 90916 | 2696 | 13017 |
Number of reflections | 21354 | ||
<I/σ(I)> | 10.6 | 38.6 | 2.3 |
Completeness [%] | 99.0 | 97.4 | 97.2 |
Redundancy | 4.3 | 3.9 | 4.2 |
CC(1/2) | 0.990 | 0.998 | 0.773 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 17% 3350, 0.2 KNaTartrate, 0.1 BTP 7.5 |