5SVI
MORC3 CW domain in complex with unmodified histone H3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-03-01 |
Detector | DECTRIS PILATUS3 R 300K |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 26.500, 31.060, 36.090 |
Unit cell angles | 107.81, 93.44, 90.21 |
Refinement procedure
Resolution | 34.290 - 1.613 |
R-factor | 0.1865 |
Rwork | 0.183 |
R-free | 0.22130 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.110 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.290 |
High resolution limit [Å] | 1.630 |
Number of reflections | 12165 |
<I/σ(I)> | 9.2 |
Completeness [%] | 86.0 |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 1.6 M sodium citrate |