5QTC
Unliganded T. brucei FPPS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-19 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 60.030, 60.030, 340.604 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 56.767 - 1.645 |
R-factor | 0.2105 |
Rwork | 0.208 |
R-free | 0.25090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | pdbid 4ryp |
Data reduction software | XDS (20180808) |
Data scaling software | Aimless (0.7.4) |
Phasing software | PHASER (2.8.2) |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.767 | 1.878 |
High resolution limit [Å] | 1.645 | 1.645 |
Rmerge | 0.092 | 1.531 |
Rmeas | 0.127 | 9.678 |
Rpim | 0.029 | 2.228 |
Total number of observations | 628869 | 92960 |
Number of reflections | 24792 | 5046 |
<I/σ(I)> | 20.3 | 0.5 |
Completeness [%] | 54.1 | 8.4 |
Redundancy | 18 | 14.5 |
CC(1/2) | 0.999 | 0.446 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 20 % w/v PEG 3350, 0.2 M sodium tartrate dibasic dihydrate |