Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5QKT

Group deposition of library data - Crystal Structure of EcDsbA after initial refinement with no ligand modelled (structure A9_1)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron siteAustralian Synchrotron
BeamlineMX1
Temperature [K]100
Detector technologyCCD
Collection date2018-04-18
DetectorADSC QUANTUM 210r
Wavelength(s)0.95370
Spacegroup nameC 1 2 1
Unit cell lengths117.148, 64.153, 74.580
Unit cell angles90.00, 126.01, 90.00
Refinement procedure
Resolution34.611 - 1.896
R-factor0.2175
Rwork0.216
R-free0.25940
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.009
RMSD bond angle1.208
Data reduction softwareXDS
Data scaling softwareAimless (0.5.32)
Phasing softwareMOLREP
Refinement softwarePHENIX (1.9_1692)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]47.38047.3801.940
High resolution limit [Å]1.9009.0901.900
Rmerge0.0530.0170.987
Rmeas0.0610.0201.138
Rpim0.0300.0100.559
Total number of observations14587212738850
Number of reflections350823412194
<I/σ(I)>12.843.91.1
Completeness [%]98.797.295.8
Redundancy4.23.74
CC(1/2)0.9990.9990.643
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.129311-13% PEG 8000 5-7.5% GLYCEROL 1 MM CUCL2 100 MM SODIUM CACODYLATE

222624

PDB entries from 2024-07-17

PDB statisticsPDBj update infoContact PDBjnumon