Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5QKB

Ground-state model of NUDT5 and corresponding apo datasets for PanDDA analysis

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04-1
Synchrotron siteDiamond
BeamlineI04-1
Temperature [K]100
Detector technologyPIXEL
Collection date2018-07-29
DetectorDECTRIS PILATUS 6M
Wavelength(s)1.000
Spacegroup nameP 1
Unit cell lengths49.074, 59.679, 80.321
Unit cell angles79.44, 81.82, 75.93
Refinement procedure
Resolution78.540 - 1.580
R-factor0.221
Rwork0.219
R-free0.25000
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)6gru
RMSD bond length0.019
RMSD bond angle1.997
Data reduction softwareXDS
Data scaling softwareAimless (0.7.1)
Phasing softwareREFMAC
Refinement softwareREFMAC (5.8.0189)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]47.32047.3201.620
High resolution limit [Å]1.5807.0701.580
Rmerge0.0320.0250.338
Rmeas0.0450.0350.478
Rpim0.0320.0250.338
Total number of observations193270233011879
Number of reflections113271
<I/σ(I)>9.8271.1
Completeness [%]95.697.493.1
Redundancy1.71.81.5
CC(1/2)0.9970.9960.813
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP293.1533 % PEG4k, 0.2 MgCl2 and 0.1 M Tris

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon