5PZV
Human liver fructose-1,6-bisphosphatase 1 (fructose 1,6-bisphosphate 1-phosphatase, E.C.3.1.3.11) complexed with the allosteric inhibitor 1-(4-bromopyridin-2-yl)-3-(4-chlorophenyl)sulfonylurea
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-04-13 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.987 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 67.618, 83.409, 277.065 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 29.672 - 2.000 |
R因子 | 0.193 |
Rwork | 0.191 |
R-free | 0.23880 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 0.910 |
Refinement software | PHENIX (1.11.1_2575) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 29.672 |
分解能 [Å] (高) | 2.000 |
独立反射数 | 100175 |
完全性 [%] | 93.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 300 | 0.1M HEPES pH 7.0, 0.1M AMMONIUM ACETATE, 12% PEG 3350 |