5PTI

STRUCTURE OF BOVINE PANCREATIC TRYPSIN INHIBITOR. RESULTS OF JOINT NEUTRON AND X-RAY REFINEMENT OF CRYSTAL FORM II

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	74.100, 23.400, 28.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 1.000
R-factor	0.2 *
RMSD bond length	0.020 *

Data quality characteristics

	Overall
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	0.940 *
Rmerge	0.049 *
Total number of observations	41385 *
Number of reflections	26499 *
Completeness [%]	76.4 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	10 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	40 (mg/ml)
2	1	drop	K-Na phosphate	0.1 (M)