Loading
PDBj
MenuPDBj@FacebookPDBj@X(formerly Twitter)PDBj@BlueSkyPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5PQU

PanDDA analysis group deposition -- Crystal Structure of BRD1 after initial refinement with no ligand modelled (structure 67)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04-1
Synchrotron siteDiamond
BeamlineI04-1
Temperature [K]100
Detector technologyPIXEL
Collection date2014-08-28
DetectorDECTRIS PILATUS 2M
Wavelength(s)0.9200
Spacegroup nameP 21 21 21
Unit cell lengths55.109, 56.248, 101.782
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.050 - 2.000
R-factor0.21
Rwork0.207
R-free0.26030
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)5amf
RMSD bond length0.016
RMSD bond angle1.658
Data reduction softwareXDS
Data scaling softwareAimless (0.3.6)
Phasing softwareREFMAC
Refinement softwareREFMAC (5.8.0131)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]29.05029.0502.050
High resolution limit [Å]2.0008.9402.000
Rmerge0.1670.0351.044
Rmeas0.1830.0391.137
Rpim0.0720.0150.441
Total number of observations13860717139187
Number of reflections21937
<I/σ(I)>13.554.52
Completeness [%]99.297.192.2
Redundancy6.35.96.3
CC(1/2)0.9930.9990.769
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP72930.1M bis-tris pH 7.0 -- 30% PEG3350

227561

PDB entries from 2024-11-20

PDB statisticsPDBj update infoContact PDBjnumon