5OYK
Outer-membrane expressed OmpT of Vibrio cholerae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 298 |
Detector technology | PIXEL |
Collection date | 2016-02-19 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.979 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 144.610, 74.330, 62.310 |
Unit cell angles | 90.00, 96.74, 90.00 |
Refinement procedure
Resolution | 46.410 - 3.200 |
R-factor | 0.21381 |
Rwork | 0.212 |
R-free | 0.24435 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ehd |
RMSD bond length | 0.011 |
RMSD bond angle | 1.528 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.410 | |
High resolution limit [Å] | 3.200 | 3.200 |
Number of reflections | 6356 | |
<I/σ(I)> | 5 | 1.5 |
Completeness [%] | 98.0 | 96 |
Redundancy | 3.6 | 3.5 |
CC(1/2) | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.5 | 298 | 15% PEG 4000 0.1 M sodium acetate 0.4 M ammonium thiocyanate |