5OXZ
Crystal Structure of NeqN/NeqC complex from Nanoarcheaum equitans at 1.2A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 78 |
| Detector technology | PIXEL |
| Collection date | 2016-12-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97929 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 45.670, 45.670, 254.412 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 42.400 - 1.200 |
| R-factor | 0.13823 |
| Rwork | 0.137 |
| R-free | 0.15628 |
| Structure solution method | AB INITIO PHASING |
| RMSD bond length | 0.033 |
| RMSD bond angle | 2.672 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | Arcimboldo |
| Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 42.410 | 1.260 |
| High resolution limit [Å] | 1.200 | 1.200 |
| Number of reflections | 51160 | |
| <I/σ(I)> | 16.2 | 4 |
| Completeness [%] | 99.9 | 99.9 |
| Redundancy | 12.2 | 12.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.1 M Di-Ammonium Tartrate pH7 |
