5OVO
Structure of DraG-GlnZ-delta42-54 complex from Azospirillum brasilense
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-07 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.91841 |
Spacegroup name | H 3 |
Unit cell lengths | 116.740, 116.740, 105.616 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.600 - 1.550 |
R-factor | 0.14505 |
Rwork | 0.144 |
R-free | 0.16453 |
RMSD bond length | 0.025 |
RMSD bond angle | 2.443 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 46.800 |
High resolution limit [Å] | 1.550 |
Rpim | 0.050 |
Number of reflections | 77898 |
<I/σ(I)> | 10.9 |
Completeness [%] | 99.8 |
Redundancy | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 298 | 35 % (v/v) glycerol ethoxylate, 0.2 M lithium citrate |