5OUT
CRYSTAL STRUCTURE OF THE FERRIC ENTEROBACTIN RECEPTOR (PFEA) MUTANT (G324V) FROM PSEUDOMONAS AERUGINOSA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-08-26 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.54178 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 87.680, 158.130, 77.880 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.080 - 2.900 |
R-factor | 0.2552 |
Rwork | 0.253 |
R-free | 0.29651 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.255 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.080 | 2.950 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.106 | 1.377 |
Number of reflections | 19876 | |
<I/σ(I)> | 12.7 | 1.4 |
Completeness [%] | 80.4 | 81.9 |
Redundancy | 3.5 | 3.5 |
CC(1/2) | 0.998 | 0.669 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 294 | PEG 8000 ADA Magnesium acetate pH 6.5 |