5OUP
Structure of TgPLP1 MACPF domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-02-28 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.0719 |
| Spacegroup name | P 65 |
| Unit cell lengths | 104.860, 104.860, 52.010 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 52.430 - 2.030 |
| R-factor | 0.193 |
| Rwork | 0.191 |
| R-free | 0.23250 |
| Structure solution method | SIRAS |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.570 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((dev_2283: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 90.810 |
| High resolution limit [Å] | 2.030 |
| Number of reflections | 21264 |
| <I/σ(I)> | 13.4 |
| Completeness [%] | 100.0 |
| Redundancy | 13.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M HEPES pH7.5, 10% isopropanol, 20% PEG 4000 |
