5OUO
Structure of TgPLP1 APCbeta domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-07-26 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9763 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 100.760, 50.210, 52.280 |
| Unit cell angles | 90.00, 90.96, 90.00 |
Refinement procedure
| Resolution | 50.370 - 1.110 |
| R-factor | 0.1501 |
| Rwork | 0.149 |
| R-free | 0.16670 |
| Structure solution method | SAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.082 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((dev_2044: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.370 |
| High resolution limit [Å] | 1.100 |
| Number of reflections | 99521 |
| <I/σ(I)> | 11.4 |
| Completeness [%] | 96.8 |
| Redundancy | 6.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 25% PEG 3350, 0.2M MgCl2, 0.1M bis-Tris, pH5.5 |
