5OO8
Streptomyces PAC13 (H42Q) with uridine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-02-17 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 66.390, 66.390, 54.841 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 57.500 - 1.780 |
R-factor | 0.16673 |
Rwork | 0.165 |
R-free | 0.19407 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.125 |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 57.500 | 1.920 |
High resolution limit [Å] | 1.780 | 1.780 |
Rmerge | 0.051 | 0.376 |
Number of reflections | 13630 | 2778 |
<I/σ(I)> | 19.2 | 3.4 |
Completeness [%] | 99.5 | 99.7 |
Redundancy | 3.6 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 0.2 M potassium sodium tartrate, 20 % w/v PEG-335 |