5OO4
Streptomyces PAC13 with uridine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-07-19 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 66.822, 66.822, 55.011 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.560 - 1.600 |
R-factor | 0.15849 |
Rwork | 0.157 |
R-free | 0.18458 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.308 |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.930 | 1.710 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.108 | |
Number of reflections | 17785 | 2281 |
<I/σ(I)> | 27.4 | 7 |
Completeness [%] | 92.5 | 67.1 |
Redundancy | 3.5 | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 15% PEG3350,0.2M NaAc,0.09MBis-Tris pH6.5 |