5ONJ

YnDL in Complex with 5 amino acid (PGA) complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-07-10
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	1.00000
Spacegroup name	P 21 21 21
Unit cell lengths	38.592, 47.651, 99.328
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.750 - 1.700
R-factor	0.169
Rwork	0.167
R-free	0.20350
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3a9l
RMSD bond length	0.006
RMSD bond angle	0.784
Data reduction software	xia2
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	15.750
High resolution limit [Å]	1.700
Number of reflections	20613
<I/σ(I)>	24.58
Completeness [%]	99.0
Redundancy	1.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291	1M Sodium Acetate, 5% gamma-PGA, 20% PEG 3350