Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5OLL

Crystal structure of gurmarin, a sweet taste suppressing polypeptide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 1
Synchrotron siteSOLEIL
BeamlinePROXIMA 1
Temperature [K]100
Detector technologyPIXEL
Collection date2014-10-10
DetectorDECTRIS PILATUS 6M
Wavelength(s)1.0332
Spacegroup nameH 3
Unit cell lengths53.650, 53.650, 38.110
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution12.000 - 1.450
R-factor0.19
Rwork0.190
R-free0.19100
Structure solution methodSAD
RMSD bond length0.010
RMSD bond angle1.130
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwareSHELXDE
Refinement softwareBUSTER (2.10.3)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0001.490
High resolution limit [Å]1.4501.450
Rmerge0.0510.800
Rpim0.0230.378
Number of reflections39858524
<I/σ(I)>18.11.9
Completeness [%]100.0100
Redundancy5.55.5
CC(1/2)0.9980.700
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.8293100 mM MES, 5 mM MgCl2, 5 mM CaCl2, 50 mM CdCl2, 50 mM NiCl2 and 12% (w/v) PEG 3350

226707

PDB entries from 2024-10-30

PDB statisticsPDBj update infoContact PDBjnumon