5OJW
S. cerevisiae UBC13 - MMs2 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-22 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.070989 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.425, 66.281, 126.614 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.780 - 2.000 |
R-factor | 0.1626 |
Rwork | 0.160 |
R-free | 0.20540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jat |
RMSD bond length | 0.011 |
RMSD bond angle | 1.035 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.780 | 1.820 |
High resolution limit [Å] | 1.773 | 1.773 |
Rmerge | 0.071 | |
Rpim | 0.056 | |
Number of reflections | 29813 | |
<I/σ(I)> | 11.1 | |
Completeness [%] | 97.6 | |
Redundancy | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.6 | 292 | 0.1M Bis-Tris Propane / Citric Acid Buffer, pH 7.6, 20% PEG3000 |