5OI9
Trichoplax adhaerens STIL N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-03-07 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.87292 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 66.020, 75.231, 68.530 |
Unit cell angles | 90.00, 97.20, 90.00 |
Refinement procedure
Resolution | 37.615 - 2.090 |
R-factor | 0.1991 |
Rwork | 0.197 |
R-free | 0.24080 |
Structure solution method | MAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.573 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | CRANK |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.620 | 2.140 |
High resolution limit [Å] | 2.090 | 2.090 |
Rmerge | 0.160 | 0.861 |
Rpim | 0.077 | 0.416 |
Number of reflections | 39751 | 3077 |
<I/σ(I)> | 7.8 | 2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 5.2 | 5.2 |
CC(1/2) | 0.993 | 0.592 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 292 | 100 mM MES pH 6.0 3 % (v/v) MPD |