5OFX
Plla lectin, trisaccharide complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-07 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.976251 |
Spacegroup name | P 1 |
Unit cell lengths | 58.979, 62.998, 75.860 |
Unit cell angles | 101.15, 112.79, 94.44 |
Refinement procedure
Resolution | 44.090 - 1.750 |
R-factor | 0.1766 |
Rwork | 0.175 |
R-free | 0.20570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l7l |
RMSD bond length | 0.005 |
RMSD bond angle | 0.738 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.090 | 1.840 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.163 | 0.773 |
Rmeas | 0.846 | |
Rpim | 0.340 | |
Number of reflections | 89118 | |
<I/σ(I)> | 8.1 | 2 |
Completeness [%] | 90.7 | 91.9 |
Redundancy | 6.1 | 6 |
CC(1/2) | 0.774 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2 M Magnesium acetate, 20 % w/v PEG 3350 |