5OCN
Crystal structure of the forkhead domain of human FOXN1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-05 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9762 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.141, 78.203, 263.479 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.913 - 2.700 |
R-factor | 0.2527 |
Rwork | 0.251 |
R-free | 0.28380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2c6y |
RMSD bond length | 0.002 |
RMSD bond angle | 0.463 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.920 | 2.830 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.101 | 1.321 |
Rmeas | 0.044 | |
Rpim | 0.713 | |
Number of reflections | 24950 | 3240 |
<I/σ(I)> | 11.8 | 1.5 |
Completeness [%] | 99.8 | 99.9 |
Redundancy | 7.1 | 7.3 |
CC(1/2) | 0.999 | 0.876 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 32 % PEG 3350, 0.25 M Potassium Citrate tribasic, 10% Ethylene Glycol |