5O9C

Crystal structure of Omp36 from Enterobacter aerogenes

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-02-20
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.917
Spacegroup name	P 3
Unit cell lengths	125.098, 125.098, 126.542
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	56.073 - 2.469
R-factor	0.1957
Rwork	0.193
R-free	0.23940
RMSD bond length	0.007
RMSD bond angle	0.965
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((1.11.1_2575: ???))

Data quality characteristics

	Overall
Low resolution limit [Å]	56.073
High resolution limit [Å]	2.460
Rmerge	0.080
Number of reflections	79038
<I/σ(I)>	9.6
Completeness [%]	99.3
Redundancy	3.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8.5	298.15	0.1 M Tris pH 8.5, 8% PEG 8000