5O78
Crystal structure of Omp35 from Enterobacter aerogenes
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-04-19 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 111.570, 115.940, 216.661 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 108.330 - 2.850 |
R-factor | 0.21597 |
Rwork | 0.214 |
R-free | 0.26034 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1omf |
RMSD bond length | 0.010 |
RMSD bond angle | 1.462 |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 108.330 | 2.920 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.110 | |
Number of reflections | 27313 | |
<I/σ(I)> | 6.3 | |
Completeness [%] | 85.0 | |
Redundancy | 2.5 | |
CC(1/2) | 0.990 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298.15 | 0.2 M Lithium Chloride, 0.05 M magnesium sulfate, 8% PEG 8000 |