5O5O
X-ray crystal structure of RapZ from Escherichia coli (P32 space group)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-05-01 |
Detector | MARRESEARCH |
Wavelength(s) | 0.87260 |
Spacegroup name | P 32 |
Unit cell lengths | 92.750, 92.750, 156.800 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.330 - 3.404 |
R-factor | 0.2041 |
Rwork | 0.197 |
R-free | 0.26630 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.323 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2747: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.330 | 3.480 |
High resolution limit [Å] | 3.400 | 3.400 |
Rmerge | 0.123 | 0.638 |
Number of reflections | 20540 | |
<I/σ(I)> | 11.2 | 1.8 |
Completeness [%] | 99.7 | 99.9 |
Redundancy | 3.5 | 3.58 |
CC(1/2) | 0.995 | 0.695 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | 0.1 M MES, 1.1 M ammonium sulfate, 0.01 M beta-mercaptoethanol, 1 percent glycerol, pH 7.0 |