5O20
Structure of Nrd1 RNA binding domain in complex with RNA (UUAGUAAUCC)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-23 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.979260 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 66.157, 66.157, 156.908 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.960 - 3.530 |
R-factor | 0.2273 |
Rwork | 0.225 |
R-free | 0.26861 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.158 |
Data reduction software | XDS |
Data scaling software | XDS |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.960 | 3.870 |
High resolution limit [Å] | 3.530 | 3.530 |
Rmerge | 0.081 | 0.435 |
Number of reflections | 4716 | 1077 |
<I/σ(I)> | 9.7 | 2.4 |
Completeness [%] | 99.5 | 99.1 |
Redundancy | 9.7 | 9.7 |
CC(1/2) | 0.990 | 0.990 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291 | 1M Sodium Potassium Phosphate pH 7.4 |