5O1Y
Structure of Nrd1 RNA binding domain in complex with RNA (GUAA)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979490 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 64.936, 64.936, 158.391 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.080 - 2.450 |
R-factor | 0.1977 |
Rwork | 0.197 |
R-free | 0.21724 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5o1w |
RMSD bond length | 0.009 |
RMSD bond angle | 1.364 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.080 | 2.550 |
High resolution limit [Å] | 2.450 | 2.450 |
Rmerge | 0.040 | 0.630 |
Rpim | 0.100 | 0.154 |
Number of reflections | 12717 | |
<I/σ(I)> | 28.2 | 3.4 |
Completeness [%] | 96.1 | |
Redundancy | 16.7 | 17.7 |
CC(1/2) | 1.000 | 0.970 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291 | 1M Sodium Potassium Phosphate pH 7.4 |