5NY8
The structure of the thermobifida fusca guanidine III riboswitch with aminoguanidine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-24 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.92019 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 83.390, 83.390, 66.330 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.955 - 2.040 |
R-factor | 0.1907 |
Rwork | 0.189 |
R-free | 0.22510 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.861 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX ((dev_2219: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.960 | 2.080 |
High resolution limit [Å] | 2.040 | 2.040 |
Rmerge | 0.049 | 1.023 |
Rpim | 0.023 | 0.462 |
Number of reflections | 32303 | 842 |
<I/σ(I)> | 16.68 | |
Completeness [%] | 99.6 | 100 |
Redundancy | 5.64 | 5.7 |
CC(1/2) | 0.999 | 0.539 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1MSodium chloride, 0.02M Magnesium chloride hexahydrate, 0.05M BisTris7.0, 30% v/vMPD |