5NR1
FzlA from C. crescentus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-06-11 |
Detector | MARRESEARCH |
Wavelength(s) | 1.54184 |
Spacegroup name | I 21 3 |
Unit cell lengths | 124.326, 124.326, 124.326 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.800 - 2.004 |
R-factor | 0.1631 |
Rwork | 0.161 |
R-free | 0.20010 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.298 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (dev_1036) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.087 | 0.448 |
Rpim | 0.043 | 0.226 |
Number of reflections | 40294 | 2792 |
<I/σ(I)> | 12.7 | |
Completeness [%] | 97.3 | 92.6 |
Redundancy | 4.9 | 4.7 |
CC(1/2) | 0.997 | 0.857 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 293 | 50% PEG 200, 0.2 M NaCl, 0.1 M sodium potassium phosphate pH 6.2 |