5NQS
Structure of the Arabidopsis Thaliana TOPLESS N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-21 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.873 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 72.681, 72.681, 181.147 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.910 - 2.610 |
R-factor | 0.2027 |
Rwork | 0.200 |
R-free | 0.24680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | partially built MAD model |
RMSD bond length | 0.010 |
RMSD bond angle | 1.090 |
Data reduction software | XDS ((VERSION January 10, 2014) |
Data scaling software | XSCALE ((VERSION January 10, 2014) |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.700 |
High resolution limit [Å] | 2.610 | 2.610 |
Number of reflections | 16949 | 10538 |
<I/σ(I)> | 12.2 | 1.79 |
Completeness [%] | 99.7 | 100 |
Redundancy | 6.8 | 6.48 |
CC(1/2) | 0.672 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | Na2HPO4-Citrate 0.2 M pH 4.2, 2-propanol 10% v/v and Lithium sulfate 0.3 M |