5NMK
HLA A02 presenting SLFNTIAVL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-05-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9778 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.840, 79.030, 58.370 |
Unit cell angles | 90.00, 116.11, 90.00 |
Refinement procedure
Resolution | 48.400 - 1.660 |
R-factor | 0.17707 |
Rwork | 0.175 |
R-free | 0.20979 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.017 |
RMSD bond angle | 1.831 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.400 | 1.700 |
High resolution limit [Å] | 1.655 | 1.655 |
Rmerge | 0.074 | 1.300 |
Number of reflections | 53961 | 4000 |
<I/σ(I)> | 9.5 | 2.1 |
Completeness [%] | 98.9 | 99.8 |
Redundancy | 3.6 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M Sodium Cacodylate, pH 6.0, 25% PEG 4000, 0.2 M Ammonium Sulphate |