5NLZ
GRIFIN (Crystallisation pH: 4.2)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-20 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.149 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.093, 60.830, 53.999 |
Unit cell angles | 90.00, 92.57, 90.00 |
Refinement procedure
Resolution | 39.054 - 1.149 |
R-factor | 0.1391 |
Rwork | 0.138 |
R-free | 0.16460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5nld |
RMSD bond length | 0.008 |
RMSD bond angle | 1.041 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.054 | 1.190 |
High resolution limit [Å] | 1.149 | 1.149 |
Rmerge | 0.024 | 0.280 |
Number of reflections | 85844 | 7759 |
<I/σ(I)> | 12.53 | 2.14 |
Completeness [%] | 95.6 | 86.82 |
Redundancy | 1.6 | 1.4 |
CC(1/2) | 0.990 | 0.820 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.2 | 295 | Crystallization condition 20% PEG 8K, 0.1M phosphate-citrate pH 4.2, 0.2M NaCl |