Experimental procedure
Temperature [K] | 263 |
Detector technology | AREA DETECTOR |
Collection date | 1992-10 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 61.480, 61.480, 70.180 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 1.750 |
R-factor | 0.186 |
Rwork | 0.186 |
RMSD bond length | 0.010 |
RMSD bond angle | 23.510 * |
Data reduction software | SDMS (DETECTOR SYSTEM (NIELSEN)) |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 1.750 |
Rmerge | 0.079 * |
Number of reflections | 14070 |
Completeness [%] | 90.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 2.5-2.8 (M) | |
2 | 1 | reservoir | Tris-HCl | or phosphate |