Experimental procedure
| Temperature [K] | 263 |
| Detector technology | AREA DETECTOR |
| Collection date | 1992-10 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 61.480, 61.480, 70.180 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 1.750 |
| R-factor | 0.186 |
| Rwork | 0.186 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 23.510 * |
| Data reduction software | SDMS (DETECTOR SYSTEM (NIELSEN)) |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 10.000 |
| High resolution limit [Å] | 1.750 |
| Rmerge | 0.079 * |
| Number of reflections | 14070 |
| Completeness [%] | 90.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 6.8 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | ammonium sulfate | 2.5-2.8 (M) | |
| 2 | 1 | reservoir | Tris-HCl | or phosphate |
