5NKX
HRSV M2-1 core domain, P3221 crystal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2016-12-06 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.03321 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 91.949, 91.949, 97.799 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.974 - 2.000 |
R-factor | 0.191709571525 |
Rwork | 0.190 |
R-free | 0.22898 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4c3e |
RMSD bond length | 0.003 |
RMSD bond angle | 0.533 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.900 | 8.970 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.052 | |
Rmeas | 0.073 | |
Number of reflections | 52178 | |
<I/σ(I)> | 6.5 | |
Completeness [%] | 97.6 | |
Redundancy | 9.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293.15 | 2.4M SODIUM MALONATE |