5N7X
CRYSTAL STRUCTURE OF STREPTAVIDIN WITH PEPTIDE EWVHPQFEQKAK
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-01 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9999 |
Spacegroup name | P 1 |
Unit cell lengths | 57.913, 64.806, 81.156 |
Unit cell angles | 96.31, 97.15, 84.09 |
Refinement procedure
Resolution | 80.130 - 1.120 |
R-factor | 0.16149 |
Rwork | 0.160 |
R-free | 0.18554 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.580 |
Data reduction software | XDS |
Data scaling software | SADABS |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.130 | 1.220 |
High resolution limit [Å] | 1.120 | 1.120 |
Rmerge | 0.031 | 0.540 |
Number of reflections | 403025 | 86936 |
<I/σ(I)> | 10.03 | 0.94 |
Completeness [%] | 90.4 | 86.1 |
Redundancy | 1.66 | 1.58 |
CC(1/2) | 0.990 | 0.370 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.1M Magnesium acetate 0.1M Sodium cacodylate pH 6.5 15% PEG6000 |