5N6X
Crystal structure of the Legionella effector WipA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9999 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 80.650, 80.650, 321.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.533 - 1.750 |
R-factor | 0.1807 |
Rwork | 0.180 |
R-free | 0.21500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | WipA411 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.844 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.533 | 1.840 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmeas | 0.077 | |
Number of reflections | 108230 | |
<I/σ(I)> | 13.94 | 1.25 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7.3 | |
CC(1/2) | 0.998 | 0.555 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.1 M Bis-Tris Propane pH7.5, 0.2 M NaBr and 20% PEG 3350 |