5N6O
Wild type human Rac1-GDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 291.15 |
Detector technology | CCD |
Collection date | 2015-07-25 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9801 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.641, 82.656, 105.898 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.590 - 2.590 |
R-factor | 0.196 |
Rwork | 0.193 |
R-free | 0.25200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.070 |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 65.158 |
High resolution limit [Å] | 2.586 |
Number of reflections | 11873 |
<I/σ(I)> | 8.4 |
Completeness [%] | 99.5 |
Redundancy | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 0,1 mM MES ph 6.5 PEG 3350 20% |