5N2W
WT-Parkin and pUB complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-04 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 147.290, 147.290, 87.490 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.340 | 2.810 |
High resolution limit [Å] | 2.680 | 2.680 |
Rmerge | 0.107 | 0.719 |
Number of reflections | 15028 | |
<I/σ(I)> | 8.9 | 1.9 |
Completeness [%] | 93.6 | 93.7 |
Redundancy | 4.6 | 4.2 |
CC(1/2) | 0.670 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 100mM Tris pH 8.5, 200mM TMAO, PEG MME 2000 |