5MYI
Convergent evolution involving dimeric and trimeric dUTPases in signalling.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-20 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97948 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 79.450, 79.450, 125.810 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 60.367 - 1.900 |
R-factor | 0.1672 |
Rwork | 0.165 |
R-free | 0.20870 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.924 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.810 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.040 | 0.390 |
Number of reflections | 19182 | 2723 |
<I/σ(I)> | 11.1 | 2.3 |
Completeness [%] | 99.9 | 100 |
Redundancy | 9.3 | 9.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 296 | 30% PEG400 0.2 M MgCl2, 0.1 M Hepes 7.5 |