5MW7
Human Jagged2 C2-EGF3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-02-02 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.92 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.814, 77.205, 96.357 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.251 - 2.800 |
R-factor | 0.2579 |
Rwork | 0.255 |
R-free | 0.31210 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4cc1 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.662 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 77.200 | 2.970 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.267 | 1.116 |
Number of reflections | 8975 | |
<I/σ(I)> | 6.2 | 1.5 |
Completeness [%] | 99.4 | 99.7 |
Redundancy | 4.8 | 5 |
CC(1/2) | 0.977 | 0.648 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 5.3 | 293 | PEG-5000 MME, Sodium citrate |