5MT4
COMPLEMENT FACTOR D IN COMPLEX WITH A REVERSIBLE BENZOIC ACID BASED INHIBITOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-10-10 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.476, 50.839, 39.366 |
Unit cell angles | 90.00, 104.93, 90.00 |
Refinement procedure
Resolution | 35.660 - 1.650 |
Rwork | 0.190 |
R-free | 0.23900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1TACE |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.600 | 1.700 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.045 | 0.273 |
Number of reflections | 25408 | |
<I/σ(I)> | 16.34 | 4.11 |
Completeness [%] | 99.1 | 99.7 |
Redundancy | 3.39 | 3.46 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 26% PEGME2000, 100mM Bis-Tris pH 6.5 |