5MT0
COMPLEMENT FACTOR D IN COMPLEX WITH A REVERSIBLE INDOLE CARBOXYLIC ACID BASED INHIBITOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-03-31 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.477, 49.527, 39.263 |
Unit cell angles | 90.00, 106.36, 90.00 |
Refinement procedure
Resolution | 29.060 - 1.290 |
Rwork | 0.154 |
R-free | 0.19600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1TACE |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.220 | 1.340 |
High resolution limit [Å] | 1.290 | 1.290 |
Rmerge | 0.045 | 0.326 |
Number of reflections | 50955 | |
<I/σ(I)> | 14.62 | 3.7 |
Completeness [%] | 98.9 | 97.6 |
Redundancy | 3.28 | 3.19 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 25% PEG3350, 100 mM BIS-TRIS pH 6.5 |