5MS9
Solution structure of Human Fibrillin-1 EGF2-EGF3-Hybrid1-cbEGF1 four domain fragment
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Home-built | OMEGA | 950 | |
| 2 | Home-built | OMEGA | 750 | |
| 4 | Bruker | AVANCE | 500 | |
| 5 | Home-built | OMEGA | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D NOESY |
| 2 | 1 | 2 | 3D 1H-15N NOESY |
| 3 | 1 | 3 | 3D 1H-13C NOESY |
| 4 | 1 | 3 | 3D 1H-13C NOESY aromatic |
| 5 | 1 | 3 | 3D 1H-13C NOESY |
| 6 | 1 | 2 | ipap |
| 7 | 1 | 3 | 3D 1H-15N NOESY |
| 8 | 1 | 4 | ipap |
| 9 | 1 | 5 | ipap |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 5.4 | 1 | 268 |
Conformers
| Conformers Calculated Total Number | 40 |
| Conformers Submitted Total Number | 20 |
