5MR9
Ligand-receptor complex.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-09-05 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.992 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 58.080, 32.750, 61.910 |
Unit cell angles | 90.00, 107.06, 90.00 |
Refinement procedure
Resolution | 48.150 - 2.400 |
R-factor | 0.25 |
Rwork | 0.248 |
R-free | 0.28850 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.060 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.400 |
Number of reflections | 8997 |
<I/σ(I)> | 6.7 |
Completeness [%] | 99.9 |
Redundancy | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 10.5 | 293 | 40% MPD and 100 mM CAPS pH 10.5. |