5MNV
Structural and functional characterization of OleP in complex with 6DEB in PEG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-10-30 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.918007 |
Spacegroup name | P 1 |
Unit cell lengths | 112.500, 116.700, 123.300 |
Unit cell angles | 103.90, 104.30, 114.70 |
Refinement procedure
Resolution | 39.970 - 2.970 |
R-factor | 0.242 |
Rwork | 0.238 |
R-free | 0.31100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.206 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 121.000 | 3.170 |
High resolution limit [Å] | 2.970 | 2.970 |
Rmerge | 0.091 | 0.486 |
Number of reflections | 101917 | |
<I/σ(I)> | 11.92 | 2.2 |
Completeness [%] | 97.5 | 91.8 |
Redundancy | 3.49 | 3.54 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 294 | 0,4M NaCl, 10mM TRIS, 22% PEG3350 |