5MN7
S. aureus FtsZ 12-316 F138A GTP Closed form (3FCm)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-03 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9282 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 116.091, 130.015, 134.125 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.677 - 3.300 |
R-factor | 0.2132 |
Rwork | 0.211 |
R-free | 0.26810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5mn5 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.505 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.480 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.098 | 0.719 |
Number of reflections | 12453 | |
<I/σ(I)> | 11.6 | 1.9 |
Completeness [%] | 91.5 | 94.3 |
Redundancy | 3.6 | 3.6 |
CC(1/2) | 0.696 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 292 | 10 mg/ml; 40% PEG monomethyl ether 350, 0.05 M MES pH 6 |