5MJL
Single-shot pink beam serial crystallography: Proteinase K
Experimental procedure
Experimental method | LAUE |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-D |
Synchrotron site | APS |
Beamline | 14-BM-D |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2016-07-10 |
Detector | RAYONIX MX340-HS |
Wavelength(s) | 1.1-1.3 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 68.300, 68.300, 108.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.108 - 2.210 |
R-factor | 0.157478947888 |
Rwork | 0.154 |
R-free | 0.19452 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5avj |
RMSD bond length | 0.002 |
RMSD bond angle | 0.571 |
Data reduction software | Precognition/Epinorm (RenzResearch) |
Phasing software | PHENIX (1.10.1-2155_9999) |
Refinement software | PHENIX (1.10.1-2155_9999) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 2.310 |
High resolution limit [Å] | 2.100 | 2.210 |
Rmerge | 0.100 | |
Number of reflections | 9197 | |
<I/σ(I)> | 18.5 | |
Completeness [%] | 57.9 | 26.06 |
Redundancy | 3.7 | 15.31 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 293 | 1.6M MgSO4, 10 mM CaCl2, 100 mM CHC buffer pH 6.5 |