5MGY
Crystal structure of Pseudomonas stutzeri flavinyl transferase ApbE, apo form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-08-27 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 1 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 135.656, 91.983, 138.061 |
| Unit cell angles | 90.00, 90.41, 90.00 |
Refinement procedure
| Resolution | 138.060 - 2.600 |
| R-factor | 0.23392 |
| Rwork | 0.232 |
| R-free | 0.27394 |
| RMSD bond length | 0.018 |
| RMSD bond angle | 2.004 |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 138.060 |
| High resolution limit [Å] | 2.600 |
| Number of reflections | 104767 |
| <I/σ(I)> | 2.7 |
| Completeness [%] | 100.0 |
| Redundancy | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 281 | 0.1 M Bis-Tris pH 6.5 28% polyethylene glycol 2000 monomethyl ether |
